E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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Testing was performed in compliance with Practice E The nitrogen is separated from other liberated gases such as hydrogen and carbon monoxide and is nally measured in a thermal conductivity cell.
Use Calibrant CCC as the primary calibrant and analyze at axtm three test samples to determine the calibration slope. Samples must be of the proper size to permit free introduction into the sample loading device, if required, and to t in the graphite crucible. In this case, laboratories should perform method validation using wstm materials. Crucibles must be composed of high purity graphite.
Please first log in with a verified email before subscribing to alerts. It is therefore recommended that calibrants be of the same or similar composition as the samples to be analyzed. NOTE 20—Although this test method was tested to only 0.
NOTE 25—For some instruments this procedure automatically precedes the analysis cycle. Use Calibrant C as the primary calibrant and analyze at least three specimens to determine the calibration slope. The preparation asym be made by flattening, cutting, diluting, casting and other equipment adaptation awtm, to fit the required size. Make a minimum of two determinations using the specimen and accelerator as directed in Upon elution, the amount of carbon dioxide is measured in ast thermistor-type conductivity cell.
Total sulfur, as SO2, is monitored and measured over a period of time.
Current edition approved October 1, NOTE 16—Repeat the calibration when: Using a clean le or water cooled silicon carbide grinding media, abrade all surfaces of the sample to remove all traces of surface oxidation or other impurities, rinse in acetone, air-dry, and weigh. Precision and Bias Add to Alert PDF.
The value should be within the allowable limits of the certied value. Standards Subsctiption may be the perfect solution. Specic hazards statements are given in Section 6.
Use crucible tongs to handle the preburned crucibles. Thin, at samples may be stamped using a punch and die. We have no amendments or corrections for this standard. Standards Subsctiption may be the perfect solution. Individual reprints single or multiple copies of this standard may be obtained by contacting ASTM at the above address or at phonefaxor service astm.
This mechanism will compensate electronically for the blank value. Preheated crucibles may also be stored in a desiccator prior to use.
No other units of measurement are included in this standard. Prepare more capsules of sulfur solution B if necessary. Originally approved in Standards Subsctiption may be the perfect solution. This distortion alters the xed capacitance creating an electric signal change that is amplied for measurement as SO2.
Thus, the absorption of IR energy can be attributed to only CO2 and its concentration is measured as changes in energy at the detector. Ni-base analyses are mainly performed as analyses of steel. Add to Alert PDF. In these cases, the removal of too much surface material e1109 cause erroneous results.
No other units of measurement are included in this standard. This standard is not included in any packages. Reports are provided according to the elements in question.
You may delete a document from your Alert Profile at any time. You may delete a document from your Alert Profile at any time. As written, this test method is not applicable to cast iron samples. The results should be within the allowable limits of the certied reference material. Nitrogen present in the sample is released as molecular nitrogen into the owing 6 Supporting data are available from ASTM International Headquarters.
E — 03 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys1 This standard is issued under the xed designation E ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision.
Make a minimum of two determinations using a specimen as directed in However, recognizing that commercial nitrogen determinators are capable of handling higher concentrations, this test method provides a calibration procedure up to 0.
The sulfur is then determined by infrared absorption. These units are commercially available. Total SO 2 is monitored and measured over a period of time.